Reaction & Storage Conditions Reaction Conditions: 1X AluI Methyltransferase Reaction Buffer Supplemented with 32 μg/ml S-adenosylmethionine (SAM) Incubate at
37°C.
1X AluI Methyltransferase Reaction Buffer: 50 mM Tris-HCl 5 mM 2-Mercaptoethanol 10 mM EDTA
pH 7.5 @ 25°C
Unit Definition: One unit is defined as the amount of enzyme required to protect 1 µg of λ DNA in 1 hour at 37°C in a total reaction volume of 10 µl against cleavage by AluI restriction endonuclease.
Protection Assay Conditions: AluI Methyltransferase is incubated with 1 µg of λ DNA in 10 µl 1X AluI Methyltransferase Buffer, supplemented with 80 µM S-adenosylmethionine, for one hour at 37°C followed by 15 minutes at 65°C. The extent of protection by AluI Methyltransferase is determined by the addition of 40 µl NEBuffer 1 supplemented with 10 mM MgCl2 and 10 units of AluI restriction endonuclease. Incubation at 37°C for 30 minutes is followed by analysis on an agarose gel.
Concentration: 5,000 units/ml
Storage Conditions: 10 mM Tris-HCl 50 mM KCl 1 mM Dithiothreitol 0.1 mM EDTA 200 µg/ml BSA 50% Glycerol
pH 7.5 @ 25°C
Storage Temperature: -20°C
Notes General notes:
Storage of SAM: S-adenosylmethionine is stored at �20°C as 32�mM solution dissolved in sulfuric acid (0.005�M) and 10% ethanol. SAM in this solution stored under ideal conditions remains active for up to 6�months. SAM is unstable at (pH 7.5), 37°C, and should be replenished for reactions incubated longer than 4 hours.
Many problems in achieving complete digestion can be alleviated by using fresh SAM.
Quality Control for Current Lot Quality control values for a specific lot can be found on the datacard which accompanies each product.
16-Hour Incubation:: Incubation of 40 units of AluI Methyltransferase with 1 μg λ DNA in 50 μl of 1X NEBuffer 2 at 37°C resulted in no detectable endonuclease contamination.
Exonuclease Activity:: Incubation of 40 units of AluI Methyltransferase with 1 μg sonicated 3H DNA (105 cpm/μg) for 4 hours at 37°C in 50 μl NEBuffer 2 released < 0.2% of the total radioactivity.